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New series of thiazoles and thiadiazines incorporated with pyrazole ring were synthesized via the reaction of 2-(1-(4-cyano-1,5-diphenyl-1H-pyrazol-3-yl)ethylidene) hydrazine-carbothioamide or 4-imino-7-methyl- 2,3-diphenyl-2H-pyrazolo[3,4-d]pyridazine-5(4H)-carbothiohydrazide with different reagents. The structures of all tautomeric forms of the newly synthesized compounds were confirmed on the basis of spectral data aided with DFT and semi-empirical calculations.

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This study is concerned with the synthesis and characterization derivatives of Thiaszolidinones 3a-e. These compounds were synthesized by reacting of thioglycolic acid with the appropriate Schiff base 2a-e, in the presence of dry benzene in moderate yields (69-73%). The structures of Thiaszolidinone were established on the basis of the spectral data like FT-IR, 1H-NMR, 13C-NMR, Gcosy and Mass.

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This review presents the up to date development of fused thiopyranothiazoles that comprise one of the thiazolidine derivatives classes. Thiazolidine and thiazolidinone-related compounds belong to the widely studied heterocycles from a medicinal chemistry perspective. From the chemical point of view, they are perfect heterodienes to undergo hetero-Diels?Alder reaction with a variety of dienophiles, yielding regio- and diastereoselectively thiopyranothiazole scaffolds. The annealing of thiazole and thiopyran cycles in condensed heterosystem is a precondition for the ?centers conservative? creation of the ligand-target binding complex and can promote a potential selectivity to biotargets. The review covers possible therapeutic applications of thiopyrano[2,3-d]thiazoles, such as anti-inflammatory, antibacterial, anticancer as well as aniparasitic activities. Thus, thiopyrano[2,3-d]thiazoles may be used as powerful tools in the development of biologically active agents and drug-like molecules.

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The review highlights the hydantoin syntheses presented from the point of view of the preparation methods. Novel synthetic routes to various hydantoin structures, the advances brought to the classical methods in the aim of producing more sustainable and environmentally friendly procedures for the preparation of these biomolecules, and a critical comparison of the different synthetic approaches developed in the last twelve years are also described. The review is composed of 95 schemes, 8 figures and 528 references for the last 12 years and includes the description of the hydantoin-based marketed drugs and clinical candidates.

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A novel approach for developing prodrugs based on masked carboxylic acids is described. Rather than using conventional esterase-based activation, thiazolidinone protecting groups have been identified that can reveal carboxylic acid groups upon activation by hydrogen peroxide. This may prove valuable in the continuing development of prodrug strategies that rely on reactive oxygen species (ROS) as a trigger. This journal is

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A series of new 4-thiazolidinone derivatives were synthesized by reacting various coumarinyl schiff bases with thioglycollic acid. The intermediate coumarinyl schiff bases were synthesized by reacting 4-hydroxyl coumarin with various substituted anilines in alcohol medium. All the newly synthesized compounds were assigned on the basis of IR,1H NMR and mass spectral data. All the newly synthesized compounds were evaluated for in-vitro antioxidant activities like DPPH, nitric oxide and hydrogen peroxide radical scavenging assay models. Most of the synthesised compounds showed good antioxidant activity.

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The present invention relates to novel amides having secondary amino groups, a process for preparing them, adducts of these amines and their uses. The amides can be prepared in a simple way from readily available starting materials. They and their adducts have, in particular, a low viscosity and are suitable as constituent of polyurethane and polyurea compositions having excellent processability and high flexibility, and also as constituent of epoxy resin compositions, in particular coatings.

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A smooth and effective protocol was proven to produce 2-amino-4-(2-hydroxy-3-methoxy-phenyl)-6-oxo-4H-thiazolo[3,2-a][1,3,5]triazine [2aTZ] via one-pot ternary condensation of easily available mercaptoacetic acid, o-vanillin and dicyandiamide along with ammonium acetate (CH3COONH4) as a catalyst. The chemical structure of the compound and its thin-film [2aTZ]TF were characterized by Fourier-Transform Infrared spectroscopy (FT-IR), Proton Nuclear Magnetic Resonance (1HNMR), Carbon Nuclear Magnetic Resonance (13CNMR), X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM) analyses. The optimization of the molecular structure, vibrational spectra and optical properties have been accomplished depends on the density functional theory (DFT) utilizing DMol3 and Cambridge Serial Total Energy Package (CASTEP) programs for [2aTZ] as the isolated molecule and crystal models. It’s very well-referred to the molecule’s structure and their contacts. They are equated with data calculated by means of various theoretical methodologies. [2aTZ]TF is fabricated by spin coating (250 ± 3 nm) and its optical properties (optical band gaps, Eg Opt, absorption index, k, reflective index, n, dielectric constant, epsilon, and optical conductivity,sigma) are also investigated. The high accurateness of the new [2aTZ] along with its suitable optical bandgap provided us to construct a photodetector and demonstrating its potential in optoelectronic implementations.

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Thiazolidinone derivatives were synthesized and their physicochemical properties are determined by absorption, H NMR spectroscopies. The third order nonlinear optical properties of thiazolidinone containing compounds were investigated in solutions using degenerate four wave mixing (DFWM) method at 532 nm.

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In this paper, we report the design, synthesis, in-silico, and in-vitro evaluations of a series of coumarin-phenylthiazole conjugates to inhibit cholinesterase enzymes. The coumarin and phenylthiazole derivatives have been synthesized separately, and further combined through covalent amine bond linkage. The synthesized compounds showed more inhibition towards BuChE than AChE, where 4-(3-bromophenyl)-1,3-thiazol-2-amine (7i) exhibited the strongest inhibition against BuChE with an IC50 value of 3.54 muM. For the conjugates, 3-[2-[4-(3-nitrophenyl)thiazol-2-ylamino]acetyl]chromen-2-one (8j) exhibited strongest inhibition with an IC50 value of 46.47 muM. The better inhibition activities towards BuChE are also shown by 3-bromo and 2-fluoro derivatives. It was also observed that the substitution at 3-position, on phenylthiazole moiety produced better results against BuChE than 4-substituted counterparts.

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